The study aimed to assess concrete characteristics and mechanical properties by incorporating pozzolan variations, heat treatments, and alkaline solution molarities. It focused on identifying the optimal pozzolan addition percentage for achieving maximum concrete strength. Specimens underwent heat treatments at 60°C, 90°C, and exposure to alkaline solutions with molarity levels of 6M for rice husk ash and 8M for palm shell ash (PSA). Compressive strength testing at 28 days revealed the most optimal strength of 25.80 MPa in concrete without heat treatment, with 10% Palm Shell Ash pozzolan addition. Non-pozzolan concrete subjected to 1 day of 90°C heat treatment exhibited a strength of 21.99 MPa. The lowest strength observed in concrete without heat treatment, with 15% rice husk ash, resulting in 12.50 MPa. FTIR analysis focused on the chemical aspects of concrete, particularly changes in molecular structure due to different parameters. Composite concrete samples incorporating rice husk ash pozzolan and varying alkaline solution concentrations showed negligible differences. Further analysis found that mixing concrete with 15% Palm shell ash without heat treatment resulted in optimal
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